Solid-State NMR Spectroscopy

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Journal Articles

Publications: (*indicates corresponding author)

Publications in international peer-reviewed scientific journals

2020

  • Overall S.A., Price L.E., Albert B.J., Gao C., Alaniva N., Judge P.T, Sesti E.L., Wender P.A., Kyei G.B., Barnes A.B. (2020), In Situ Detection of Endogenous HIV Activation by dynamic Nuclear Polarization NMR and Flow Cytometry. International Journal of Molecular Sciences. 21, 4649. external page doi: 10.3390/ijms21134649.
  • Osborn-Popp T., Däpp A., Gao C., Chen P.H, Price L.E., Alaniva N., Barnes A.B. (2020), Highly stable magic angle spinning spherical rotors. Magnetic Resonance. 1. 97-103. 10.5194/mr-1-97-2020. external page doi: 10.1021/acs.jpcb.9b10494
  • Judge P.T, Sesti E.L., Price L.E., Albert B.J, Alaniva N., Saliba E.P., Halbritter T., Sigurdsson S.T., Kyei G.B., Barnes A.B. (2020), Dynamic Nuclear Polarization with Electron Decoupling in Intact Human Cells and Cell Lysates. J. Phys. Chem. B. 124 (12), 2323-2330. external page doi: 10.1021/acs.jpcb.9b10494.

2019

  • Judge P.T., Sesti E.L., Alaniva N., Saliba E.P., Price L.E., Gao, C., Halbritter T., Sigurdsson S.T., Kyei G.B., Barnes A.B. (2019), Characterization of Frequency-chirped Dynamic Nuclear Polarization in Rotating Solids. Journal of Magnetic Resonance. external page doi:10.1016/j.jmr.2020.106702.
  • Judge P.T., Sesti E.L., Price L.E., Albert B.J., Alaniva N., Saliba E.P., Halbritter T., Sigurdsson S.T., Kyei G.B., Barnes A.B. (2019), Dynamic nuclear polarization with electron decoupling in intact human cells and cell lysates. The Journal of Physical Chemistry B. external page doi:10.1021/acs.jpcb.9b10494
  • Gao C., Alaniva N., Saliba E.P., Sesti E.L., Judge P.T, Scott F.J., Halbritter T., Sigurdsson S.T., Barnes A.B. (2019), Frequency-chirped dynamic nuclear polarization with magic angle spinning using a frequency-agile gyrotron. Journal of Magnetic Resonance. external page doi:10.1016/j.jmr.2019.106586.
  • Chen, P. Gao, C., Barnes A.B. (2019), Perspectives on microwave coupling into cylindrical and spherical rotors with dielectric lenses for magic angle spinning dynamic nuclear polarization. Journal of Magnetic Resonance 308, 106586. external page doi.org/10.1016/j.jmr.2019.07.005.
  • Saliba E.P., Barnes A.B. (2019), Fast electron paramagnetic resonance magic angle spinning simulations using analytical powder averaging techniques. The Journal of Chemical Physics 151, 114107. external page doi.org/10.1063/1.5113598.
  • Judge, P.T., Sesti, E.L., Saliba, E.P., Alaniva, N., Halbritter, Th., Sigurdsson, S.Th., Barnes, A.B. (2019), Sensitivity analysis of magic angle spinning dynamic nuclear polarization below 6 K. Journal of Magnetic Resonance, 305, 51-57. external page doi.org/10.1016/j.jmr.2019.05.011.
  • Alaniva N., Saliba E.P., Sesti E.L., Judge P.T., Barnes A.B. (2019), Electron decoupling with chirped microwave pulses for rapid signal acquisition and electron saturation recovery. Angewandte Chemie, 58, 7259-62. external page doi:10.1002/anie.201900139.
  • Gao C., Judge P.T., Sesti E.L., Price L., Alaniva N., Saliba E.P., Albert B.J., Soper N. J., Chen P.W., Barnes A.B. (2019), Four millimeter spherical rotors spinning at 28 KHz with double-saddle coils for cross polarization NMR. Journal of Magnetic Resonance, 303, 1-6. external page doi:10.1016/j.jmr.2019.03.006.

 

After WUSTL faculty appointment

2018

  • Scott F.J., Alaniva N., Sesti E.L., Golota N.C., Albert B.J., Price L., Chen P.W., Gao C., Saliba E.P., O’Connor R.D., Barnes A.B.* (2018). A versatile cryostat for dynamic nuclear polarization NMR supports multiple cryogenic magic angle spinning transmission line probes. Submitted to Journal of Magnetic Resonance. external page doi.org/10.1016/j.jmr.2018.10.002
  • Chen P.W., Albert B.J., Gao C, Alaniva N., Price L., Scott F. J., Saliba E.P., Sesti E.L., Fisher E.W., Barnes A.B.* (2018). Magic angle spinning spheres. Science Advances. Accepted July 25th, in press. external page 10.1126/sciadv.aau1540
  • Saliba E.P., Golota N.C., Sesti E.L., Alaniva N., Scott F.J., Albert B.J., Chen P.W., Barnes A.B.* (2018). Pulsed electron decoupling and time domain dynamic nuclear polarization with chirped microwave pulses. Perspective article in Journal of Physical Chemistry Letters. Accepted, in press for special issue. external page doi.org/10.1021/acs.jpclett.8b01695
  • Sesti E.L., Saliba E.P., Alaniva N., Albert B.J., Scott F.J., Barnes A.B.* (2018) Electron decoupling with cross polarization and dynamic nuclear polarization <6 K. Journal of Magnetic Resonance. Accepted, in press. external page doi: 10.1016/j.jmr.2018.07.016
  • Albert B.J., Gao C., Sesti E.L., Saliba E.P., Alaniva N., Scott F.J., Barnes A.B.* (2018) Dynamic nuclear polarization NMR in human cells using fluorescent polarizing agents. Biochemistry. Accepted, in press. external page doi:10.1021/acs.biochem.8b00257
  • Scott F.J., Sesti E.L., Choi E.J., Saliba E.P., Albert B.J., Laut A.J., Sirigiri J.R., Barnes A.B.* (2018) Magic angles spinning NMR with metallized rotors as cylindrical microwave resonators. Magnetic Resonance Chemistry. (January) 1-5. external page doi: 10.1002/mrc.4744
  • Scott F.J., Saliba E.P., Albert B.J., Alaniva N., Sesti E.L., Gao C., Golota N.C., Choi E.J., Jagtap A.P., Wittmann J., Eckardt M., Harneit W., Corzilius B., Sigurdsson S., Barnes A.B.* (2018) Frequency-agile gyrotron for electron decoupling and pulsed dynamic nuclear polarization. Journal of Magnetic Resonance. 289, 45-54. external page doi.org/10.1016/j.jmr.2018.02.010
  • Yang H., Staveness D., Ryckbosch S.M., Axtman A.D., Loy B.A., Barnes A.B., Pande V.S., Schaefer J., Wender P.A., Cegelski L. (2018) REDOR NMR Reveals Multiple Conformers for a Protein Kinase C Ligand in a Membrane Environment. ACS Central Science, 4, 89-96. external page doi.org/10.1021/acscentsci.7b00475
  • Sesti E.L., Alaniva N., Rand P.W., Choi E.J., Albert B.J., Saliba E.P., Scott F.J., Barnes A.B.* (2018) Magic angle spinning NMR below 6 K with a computational fluid dynamics analysis of fluid flow and temperature gradients. Journal of Magnetic Resonance, 286, 1-9.  external page doi: 10.1016/j.jmr.2017.11.002

2017

  • Albert B., Pahng S., Alaniva N., Rand P.W., Sesti E.L., Saliba E.P., Scott F., Choi E.J., Barnes A.B.* (2017) Instrumentation for cryogenic magic angle spinning dynamic nuclear polarization using 90 L of liquid nitrogen per day. Journal of Magnetic Resonance, 283, 71-78. external page doi.org/10.1016/j.jmr.2017.08.014
  • Albert B., Niu A., Ramini R., Marshall G., Wender P.A., Williams R.M., Ratner L., Barnes A.B.*, Kyei G.B.* (2017) Combinations of isoform-targeted histone deacetylase inhibitors and bryostatin analogs display remarkable potency to activate latent HIV without global T-cell activation. Scientific Reports, 7, 7456. external page doi: 10.1038/s41598-017-07814-4. PMCID: PMC5547048
  • Saliba E.P., Sesti E.L, Scott F.J., Albert B.J., Choi E.J., Alaniva N., Gao C., Barnes A.B.* (2017) Electron decoupling with dynamic nuclear polarization in rotating solids. Journal of the American Chemical Society, 139(18), 6310-6313. external page doi: 10.1021/jacs.7b02714
  • Ni Q.Z, Markhasin E, Can T.V, Corzilius B, Tan KO, Barnes A.B, Daviso E, Griffin R.G. (2017) Peptide and protein dynamics and low-temperature/DNP magic angle spinning NMR. The Journal of Physical Chemistry B, 121 (19), 4997 -5006. external page doi.org/10.1021/acs.jpcb.7b02066

2015

  • Hoff D.E., Albert B.J., Saliba E.P., Scott F.J., Choi, E.J., Mardini M., Barnes A.B.* (2015) Frequency swept microwaves for hyperfine decoupling and time domain dynamic nuclear polarization. Solid State Nuclear Magnetic Resonance, 72, 79-89. external page doi: 10.1016/j.ssnmr.2015.10.001. PMCID: PMC4762658
     

Published prior to Washington University in St. Louis

2013

  • Jawla S., Ni Q.Z., Barnes A.B., Guss W., Daviso E., Herzfeld J., Griffin R.G., Temkin R.J. (2013) Continuously tunable 250 GHz gyrotron with a double disk window for DNP-NMR spectroscopy. Journal of Infrared, Millimeter and Terahertz Waves, 34, 42-52. PMCID: PMC3607393 external page doi: 10.1007/s10762-012-9947-1

2012

  • Barnes A.B., Markasin E., Daviso E., Michaelis V.K., Mena E., DeRocher, R., Thakkar A., Nanni E.A., Jawla S., Woskov P., Herzfeld J., Temkin R.J., Griffin R.G. (2012) Dynamic nuclear polarization at 700 MHz/460GHz. Journal of Magnetic Resonance, 224, 1-7. (Cover Article) PMCID: PMC3965575  external page doi: 10.1016/j.jmr.2012.08.002
  • Barnes A.B., Nanni A. N, Herzfeld, J., Griffin R.G., Temkin R.J. (2012) A 250 GHz gyrotron with a 3 GHz tuning bandwidth for dynamic nuclear polarization. Journal of Magnetic Resonance, 221, 147-153. PMCID: PMC3405196 external page doi.org/10.1016/j.jmr.2012.03.014
  • Smith A.A., Corzilius B., Barnes A.B., Maly T., Griffin R.G. (2012) Solid effect dynamic nuclear polarization and polarization pathways. Journal Chemical Physics, 136, 015101. PMCID: PMC3265031 external page doi.org/10.1063/1.3670019

2011

  • Corzilius B., Smith A.A., Barnes A.B., Luchinat C., Bertini I., Griffin R.G. (2011) High field dynamic nuclear polarization with high-spin transition netal ions. Journal American Chemical Society, 133, 5648-5651. PMCID: PMC3086350 external page doi.org/10.1021/ja1109002
  • Nanni E.A., Barnes A.B., Matsuki Y., Woskov P., Corzilius B., Griffin R.G., Temkin R.J. (2011) Microwave field distribution in a magic angle spinning dynamic nuclear polarization probe. Journal of Magnetic Resonance, 210, 16-23. PMCID: PMC308142 external page doi: 10.1016/j.jmr.2011.02.001.
  • Nanni E.A., Barnes A.B., Griffin R.G., Temkin R.J. (2011) THz dynamic nuclear polarization NMR. IEEE Transactions on Terahertz Science and Technology, 1, 145-163. external page doi: 10.1109/TTHZ.2011.2159546

2010

  • Debelouchina G., Bayro M., van der Wel P., Caporini M., Barnes A.B., Rosay M., Maas W., Griffin R.G. (2010) Dynamic nuclear polarization-enhanced solid-state NMR spectroscopy of GNNQQNY nanocrystals and amyloid fibrils. Physical Chemistry Chemical Physics, 12, 5911-5919. PMCID: PMC4440577 external page doi: 10.1039/c003661g
  • Torrezan A.C., Han S-T., Mastovsky I., Shapiro M.A., Sirigiri J.R., Temkin R.J., Barnes A.B., Griffin R.G. (2010) Continuous-wave operation of a frequency-tunable 460-GHz second-harmonic gyrotron for enhanced nuclear magnetic resonance. IEEE Transactions on Plasma Science, 38, 1150-1159 external page doi: 10.1109/TPS.2010.2046617

2009

  • Barnes A.B., Andreas L.B., Huber M., Ramachandran R., van der Wel P.C.A., Veshtort M., Griffin R.G., Mehta M.A. (2009) High-resolution solid-state NMR structure of alanyl-prolyl-glycine. Journal of Magnetic Resonance, 200(1), 95-100. PMCID: PMC4133121 external page doi.org/10.1016/j.jmr.2009.06.009
  • Barnes A.B., Mak-Jurkauskas M.L., Matsuki Y., Bajaj V.S., van der Wel P.C.A., DeRocher R., Bryant J., Sirigiri J.R., Temkin R.J., Lugtenburg J., Herzfeld J., Griffin R.G. (2009) Cryogenic sample exchange NMR probe for magic angle spinning dynamic nuclear polarization. Journal of Magnetic Resonance, 198(2), 261-270. (Cover Article) PMCID: PMC2957365external page doi.org/10.1016/j.jmr.2009.03.003

2006

  • Bertmer M., Nieuwendaal R.C., Barnes A.B., Hayes S.E. (2006) Solid-state photodimerization kinetics of alpha-trans-cinnamic acid to alpha-truxillic acid studied via solid-state NMR. Journal of Physical Chemistry B, 110 (12), 6270-6273. external page doi: 10.1021/jp057417h
  • Calhoun A., Nicholson P., Barnes A.B. (2006) The use of inverse gas chromatography to study surface thermal oxidation of polypropylene. Polymer Degradation and Stability, 91(9), 1964-1971. external page doi.org/10.1016/j.polymdegradstab.2006.02.015

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